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Ioka, Ikuo; Kuriki, Yoshiro*; Iwatsuki, Jin; Kubo, Shinji; Inagaki, Yoshiyuki; Sakaba, Nariaki
no journal, ,
IS process is one of candidates for the large-scale production of hydrogen. Severe corrosive environment which is thermal decomposition of sulfuric acid exists in the IS process. A hybrid material with the corrosion-resistance and the ductility was made by a plasma spraying and laser treatment. The specimen had excellent corrosion resistance in the condition of 95% boiling sulfuric acid. On the other hand, the corrosion rate of the specimen in 47% boiling sulfuric acid was fifty times higher than that in 95% boiling sulfuric acid. It seems that the cracks of the surface layer weren't sealed up perfectly in the condition of 47% boiling sulfuric acid. To improve the corrosion resistance of the specimen in 47% boiling sulfuric acid, the specimen was treated with a thermal treatment for pre-oxidation. The pre-oxidized specimen got superior corrosion resistance in the condition of 47% boiling sulfuric acid. It was confirmed that the pre-oxidation was effective in improving corrosion resistance of the specimen.
Komatsu, Atsushi; Saito, Shigeru; Obayashi, Hironari; Kita, Satoshi*; Igarashi, Takahiro
no journal, ,
Corrosion tests were conducted on SUS316L and T91 in molten lead-bismuth eutectic (LBE) alloy under flow with oxygen concentration of 10wt% to investigate the effects of pre-oxidation (steam oxidation and oxidation in oxygen-saturated LBE) on corrosion. The corrosion inhibition effect was observed for both pre-oxidation treatments, and the corrosion inhibition effect increased when these pre-oxidation treatments were combined.